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Beilstein J. Org. Chem. 2012, 8, 819–826, doi:10.3762/bjoc.8.91
Graphical Abstract
Figure 1: Amines used for the synthesis of glycoclusters.
Scheme 1: Synthesis of glycocluster B5 with isolation of the intermediate diazide 2.
Scheme 2: Deacetylation of glycoconjugates B1–B6. (a) NaOMe, MeOH.
Scheme 3: Formation of side-product 5 during the synthesis of 4.
Figure 2: Dose-response curves for the inhibition of binding of HRP-labeled WGA to covalently immobilized Glc...
Figure 3: Molecular model of divalent ligand C4 with its two chitobiose moieties occupying two adjacent bindi...